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| Determination of the Migration of Banned Aromatic Amines in Paper Packaging Materials for Foodstuffs Using Gas Chromatography-tandem Mass Spectrometry |
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| DOI：10.11980/j.issn.0254-508X.2011.11.002 |
| Key Words:paper packaging materials for foodstuffs banned aromatic amines gas chromatography-tandem mass spectrometry |
| Author Name | Affiliation | | 王成云 | 深圳出入境检验检疫局,广东深圳,518045 | | 杨左军 | 深圳出入境检验检疫局,广东深圳,518045 | | 谢堂堂 | 深圳出入境检验检疫局,广东深圳,518045 | | 沈雅蕾 | 深圳出入境检验检疫局,广东深圳,518045 | | 张恩颂 | 深圳出入境检验检疫局,广东深圳,518045 | | 刘彩明 | 深圳出入境检验检疫局,广东深圳,518045 |
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| Abstract:In this paper, an effective method for determination of the migration of banned aromatic amines in paper packaging materials for foodstuffs using gas chromatography-tandem mass spectrometry (GC/MS-MS) was established. The sample was first extracted by deionized water, the extract was then concentrated on a solid phase extraction column and eluted by methanol. The elution was condensed and solved in methanol for GC/MS-MS analysis. The analyte was detected by triple quadrupole MS in multi-reaction monitoring (MRM) mode. The recoveries were in the range of 63.1%~98.4% while the relative standard deviation (RSD) changed from 2.6% to 16.2%. The limit of detection was lower than 1.0 ng/mL for all 24 kinds of banned aromatic amines at the condition of S/N=10. |
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