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草浆黑液磷酸酸析最佳条件和肥料特性的研究
Optimal Conditions of Lignin Precipitation from Straw Pulping Black Liquor by Using Phosphoric Acid
收稿日期：  
DOI：10.11980/j.issn.0254-508X.2013.02.017
关键词:  磷酸  草浆黑液  酸析  木素
Key Words:phosphoric acid  straw pulping black liquor  precipitate  lignin
基金项目:
作者单位
江启沛1 1.保定市环境保护研究所, 河北保定，071051 
王富伟2 2.保定市清漪环保科技服务中心，河北保定，071051 
张　越1 1.保定市环境保护研究所, 河北保定，071051 
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摘要:应用磷酸溶液对麦草浆黑液进行木素酸析沉淀反应，对不同pH值下的酸析木素进行了紫外光谱和红外光谱分析，并对沉淀出的酸析木素进行成分分析。实验结果表明，磷酸对麦草浆黑液酸析沉淀的最佳工艺条件为：pH值3，温度60℃，在此工艺条件下酸析木素得率为87%。紫外光谱与红外光谱分析表明，pH值降低有利于酸析木素得率的提高。酸析木素成分分析表明，酸析木素中游离腐植酸较高，是很好的肥料载体。
Abstract:A process using phosphoric acid to precipitate lignin from straw pulping black liquor was investigated, the conditions were optimized, as pH=3, T=60℃, the yield of the precipitated lignin was 87%. The precipitated lignins at different pH were analyzed by infrared spectrum and ultraviolet spectral. The components of acid-precipitated lignin at pH=3 was analyzed, the result indicated that the precipitated lignin has the characteristic of fertilizer.
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